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Sintesis Hidroksiapatit dari Precipitated Calcium Carbonate (PCC) Cangkang Telur Ayam Ras melalui Proses Presipitasi

机译:沉淀法从沉淀碳酸钙(PCC)肉鸡壳中合成羟基磷灰石

摘要

Hydroxyapatite is high biactive dan bioafinity ceramic materials. Hydroxyapatite also known osteoconductive, non-toxic, and non-immunogeic. So that there are many application ofhydroxyapatite such as catalyst, fertilizer industry and pharmacy product, protein cromatography application, water treatment, bone and teeth repair. In this research, hydroxyapatite synthesised from PCC of chicken\u27s egg shell by using precipitation methodwith variation of pH (9, 10, and 11) and stirring speed (200, 250, and 300 rpm). Hydroxyapatite that acquired has been analyze by using FTIR, XRD, SEM-EDX, dan BET. From FTIR analysis best hydroxyapatite acquired by synthesis using pH 11 for stirring speed200 rpm, pH 9 for stirring speed 250 rpm, and pH 11 for stirring speed 300 rpm. From XRD analysis acquired hydroxyapatite with best crystalinity if it comparred with standardhydroxyapatite and smallest crystal size in pH 11 and stirring speed 300 rpm that is 23,07 nm. From SEM-EDX analysis known that acquired hydroxyapatite from synthesis in pH 11and stirring speed 300 rpm has agglomarate shape with particle size 62,5 nm and molar ratio 1,41. The result of BET analysis show that total surface area of hyroxyapatite was 28,406m2/g
机译:羟基磷灰石是高双活性丹生物亲和陶瓷材料。羟基磷灰石还已知具有骨传导性,无毒和非免疫性。因此,羟基磷灰石有许多用途,例如催化剂,肥料工业和制药产品,蛋白质cromatography应用,水处理,骨骼和牙齿修复。本研究采用pH值(9、10和11)和搅拌速度(200、250和300 rpm)变化的沉淀法,从鸡卵壳的PCC中合成羟基磷灰石。通过使用FTIR,XRD,SEM-EDX和dan BET对获得的羟基磷灰石进行了分析。从FTIR分析中,通过使用pH 11用于搅拌速度200 rpm,pH 9用于搅拌速度250 rpm和pH 11用于搅拌速度300 rpm合成得到的最佳羟基磷灰石。根据XRD分析,如果与标准羟基磷灰石相比,且在pH 11和300 rpm的搅拌速度(23.07 nm)下具有最小的晶体尺寸,则可获得结晶度最佳的羟基磷灰石。根据SEM-EDX分析,已知在pH 11和搅拌速度300 rpm下通过合成获得的羟基磷灰石具有团聚体形状,粒径为62.5nm,摩尔比为1.41。 BET分析的结果表明,羟磷灰石的总表面积为28,406m2 / g

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